簡介
CO-3EBATTC_CC-18
可選擇電解質種類:
可選擇電極直徑:
介紹
應用說明
該電池可用於所有常見的電池測量,如恒電流循環、循環伏安法或電化學阻抗頻譜。液體和固態或凝膠聚合物的電解質都可以被研究。此外,還可以研究超級電容器材料的特性和性能。可以檢查各種材料,包括典型的鋰離子電極(石墨、NMC、LTO等)和其它化學材料—鈉、鎂、鉀…。它還可以應用於測量隔板和電解質的離子電導率。由於有螺旋測微器的控制旋鈕,可以研究施加在電池上的初始壓力與固態電解質或高容量負極材料技術(無負極(Anode-free)電池)的性能之間的關係。
上圖顯示了施加到電極堆的壓力與從接觸點移動的距離之間的關係。接觸點可以通過檢查 OCV(參見以下影片)或通過計算來確定。要計算接觸點,請從 4 mm 中減去電極堆疊厚度。例如,對於 0.9 mm的堆疊,接觸點(即螺旋測微器螺絲上的數值)將為 4 mm—0.9 mm = 3.1 mm。因此,您應該把螺旋測微器的螺絲調到3.1 mm,從這一點開始測量距離/壓力關係。
技術規格
產品包括
Select electrolyte type:
Select elelctrode diameter:
description
This cell is designed as high-quality alternative to Swagelok-type constructions for reproducible electrochemical measurements of battery and supercapacitor materials. The cell consists of two main elements: (i) the cell base with micrometre screw and compression spring, which allows precise control of pressure applied to the electrode sandwich; and (ii) electrode cartridge where the anode, cathode and reference electrode are located. The (default) electrode cartridge and plungers are designed for planar electrodes with diameter of 18 mm and total sandwich thickness of 2.5 mm. The diameter of separator shall be at least 2 mm larger than electrode diameter (max. 22 mm). The lock ring secures the separator in the electrode cartridge allowing easy and safe electrodes insertion, while ensuring accurate alignment. The upper and lower electrode plungers are available in various materials: 316L Stainless Steel (default), copper, aluminum, nickel etc. The pin-type reference electrode is installed from the side of the electrode cartridge. Thanks to sharp edged hole at the end of the pin the reference electrode (Li/Na/K etc.) can be easily punched from the metal foil and directly loaded into cell. The magnetic mount facilitates rapid assembly of the cartridge in the cell base. The force applied to the electrodes can reach up to 90N and is adjusted with the micrometer control knob. For 2-electrode measurements the reference electrode feedthrough hole can be closed with the reference electrode punch.
The cell elements are constructed with materials that are inert to the sample (Stainless steel and PEEK). It well fits aqueous (FKM and EPDM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. Good electrical contact is ensured by gold plated pins. The construction is gas-tight and can be effortlessly assembled in the glove box, reducing possible human error to minimum.
Application note
This cell can be used for all common battery measurements, such as galvanostatic cycling, cyclic voltammetry or electrochemical impedance spectroscopy. Both liquid and solid-state or gel-polymer electrolytes can be studied. Additionally, properties and performance of supercapacitor materials can be investigated. Various materials can be examined, including typical Li-ion electrodes (graphite, NMC, LTO etc.) and other chemistries – sodium, magnesium, potassium etc. It can also be applied to measure the ionic conductivity of separators and electrolytes. Owing to the micrometer control knob, the relationship between the initial pressure applied to the cell and the performance of solid-state electrolytes or metal plating process (anode-free systems) can be studied.
The above graph shows relation of pressure applied to electrode stack and distance travelled from the point of contact. The point of contact can be determined by checking OCV (see manual video) or by calculation. To calculate the point of contact, subtract electrode stack thickness from 4 mm. For example, for the 0.9 mm stack, the point of contact (i.e. reading on micrometer screw) will be 4 mm – 0.9 mm = 3.1 mm. Therefore, you should set micrometer screw to 3.1 mm and measure distance/pressure relation from this point.
Specification
Product includes