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電池盒—溫度監控
BATTERY CARTRIDGE – TEMPERATURE MONITORING

【Redox.me】電化學周邊耗材 電池和超級電容器

電池盒—溫度監控

簡介

CTG-A-TM_3ES-18

該測試盒在三電極電池測試單元的基礎上,加入了測量電極堆附近溫度的功能。當研究人員想在控制壓縮條件下對電池和超級電容器材料進行可重複的電化學測量時,它是理想的選擇。安裝的溫度感測器是標準的Pt100電阻溫度計(RTD)。它確保了在-50°C → +250°C範圍內的準確和可靠的讀值。具有堅固的結構,感測元件被封裝在一個堅固的316不銹鋼護套中,而導線是兼具耐用和可撓性的Teflon絕緣,並有屏蔽層,以防止電磁干擾,可連接到任何2、3或4線的Pt100溫度量測設備中。溫度探針位於參考電極邊上,與電解質直接接觸,確保從電池內部獲得精確和真實的溫度讀值。

我要諮詢

選擇電解液類型:
有機電解質 
水性電解質 

選擇電極直徑:
18mm(標準)
12mm
15mm
16mm

介紹
該測試盒在三電極電池測試單元的基礎上,加入了測量電極堆附近溫度的功能。當研究人員想在控制壓縮條件下對電池和超級電容器材料進行可重複的電化學測量時,它是理想的選擇。安裝的溫度感測器是標準的Pt100電阻溫度計(RTD)。它確保了在-50°C → +250°C範圍內的準確和可靠的讀值。具有堅固的結構,感測元件被封裝在一個堅固的316不銹鋼護套中,而導線是兼具耐用和可撓性的Teflon絕緣,並有屏蔽層,以防止電磁干擾,可連接到任何2、3或4線的Pt100溫度量測設備中。溫度探針位於參考電極邊上,與電解質直接接觸,確保從電池內部獲得精確和真實的溫度讀值。

  • 電池盒—溫度監測由上下電極柱塞、隔板鎖環、參考電極沖頭和溫度探針(Pt100)組成。
  • 附的標準電極柱塞是為直徑為18 mm、總夾層厚度達2.5 mm的平面電極設計。
  • 隔板的直徑應至少比電極直徑大 2 mm(最大 22 mm)。鎖環將隔板固定在電極盒中,使電極的插入更加容易和安全,同時確保准確對準。
  • 上、下電極柱塞有多種材料可供選擇:316L不銹鋼(標準)、銅、鋁、鎳等。
  • 針式參考電極從電極盒的側面安裝。由於針腳末端有尖銳的邊緣孔,參考電極(Li/Na/K等)可以很容易地從金屬箔上打孔下來,直接裝入電池。
  • 對於雙電極測量,可以使用參考電極沖頭封閉參考電極饋通孔。
  • 電池元件是用對樣品有惰性的材料(不銹鋼和PEEK)製成的。它很適合水性(FKM和EPDM O形環)和有機溶劑(FFKM O形環)的電解質要求。鍍金針腳可確保良好的電氣接觸。該結構是氣密性的,可以毫不費力地在手套箱中進行組裝,將可能的人為錯誤降到最低。

應用說明
該電池可用於所有常見的電池測量,如恒電流循環、循環伏安法或電化學阻抗頻譜。液體和固態或凝膠聚合物的電解質都可以被研究。此外,還可以研究超級電容器材料的特性和性能。可以檢查各種材料,包括典型的鋰離子電極(石墨、NMC、LTO等)和其它化學材料 - 鈉、鎂、鉀…。它還可以應用於測量隔板和電解質的離子電導率。Pt100溫度感測器增加了量測過程中蒐集即時溫度數據的選項。

規格

  • 推薦電極直徑:18 mm(其他選項:12 mm、15 mm、16 mm)
  • 推薦最小隔板直徑:電極直徑 + 2 mm(最大 22 mm)
  • 最大電極夾層厚度:2.5 mm
  • 工作溫度:-40°C – 80°C 

Pt100溫度感測器規格

  • 感測器類型 : Pt100(100 Ω @ 0°C),符合IEC751標準,B級,4線
  • 結構:直徑3 mm,316不銹鋼護套
  • 溫度範圍:-50°C至+250°C
  • 延長電纜:2 M的可撓性的Teflon®遮蔽絕緣
  • 終端:4線末端-允許連接到任何PT100儀器的2、3或4線(根據要求可訂購DB9連接器)

產品包括

  • 1x帶溫度感測器界面的三電極盒
  • 1x Pt100 溫度感測器
  • 1x參考電極沖頭
  • 1x上柱塞(不銹鋼316L/317L)
  • 1x下柱塞(不銹鋼316L/317L) 
  • 1x隔板鎖環 
  • 1 x O 形環
  • 1 x 溫度感測器支架

Select electrolyte type:

  • organic electrolyte
  • water-based electrolyte

Select elelctrode diameter:

  • 18 mm(default)
  • 12 mm
  • 15 mm
  • 16 mm

This cartridge incorporates ability to measure temperature near the electrode stack to the features of the Three Electrode Battery Test Cell. It is ideal choice when researcher wants to monitor temperature while performing reproducible electrochemical measurements of battery and supercapacitor materials under controlled compression. The installed temperature sensor is standard Pt100 resistance temperature detector (RTD). It ensures accurate and reliable readings in -50°C → +250°C range. It has a robust construction with the sensing element encased in a rigid 316 stainless steel sheath. The leads have a durable and flexible Teflon insulation and are screened for protection against electromagnetic interference. Leads connect to any 2, 3 or 4 wire Pt100 temperature measuring equipment. The temperature probe is located next to the reference electrode and is in direct contact with electrolyte, ensuring precise and real temperature reading from inside the cell.

The Battery Cartridge – Temperature Monitoring consists of upper and lower electrode plungers, separator lock ring, reference electrode punch and temperature probe (Pt100). The (default) electrode plungers are designed for planar electrodes with diameter of 18 mm and total sandwich thickness up to 2.5 mm. The diameter of separator shall be at least 2 mm larger than electrode diameter (max. 22 mm). The lock ring secures the separator in the electrode cartridge allowing easy and safe electrodes insertion, while ensuring accurate alignment. The upper and lower electrode plungers are available in various materials: 316L/317L Stainless Steel (default), copper, aluminium, nickel, gold plated nickel, etc. The punch-type reference electrode is installed from the side of the electrode cartridge. Thanks to sharp edged hole at the end of the pin the reference electrode (Li/Na/K etc.) can be easily punched from the metal foil and directly loaded into cell. The magnetic mount facilitates rapid assembly of the cartridge in the cell base For 2-electrode measurements the reference electrode feedthrough hole can be closed with the reference electrode punch.
The battery cartridge elements are constructed with materials that are inert to the sample (Stainless steel 316L/317L and PEEK). It well fits aqueous (FKM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. Good electrical contact is ensured by gold plated pins. The battery cartridge can be effortlessly installed in the Three Electrode Battery Test Cell even when operating in the glove box, reducing possible human error to minimum.

Application note 
This cell can be used for all common battery measurements, such as galvanostatic cycling, cyclic voltammetry or electrochemical impedance spectroscopy. Both liquid and solid-state electrolytes can be studied. Additionally, properties and performance of supercapacitor materials can be investigated. Various materials can be examined, including typical Li-ion electrodes (graphite, NMC, LTO, etc.) and other chemistries – sodium, magnesium, potassium etc. It can also be applied to measure the ionic conductivity of separators and electrolytes. The Pt100 temperature sensor adds option to collect real-time temperature data during measurement.

Specification 
default electrode diameter: 18 mm (other options: 12 mm, 15 mm, 16 mm)
recommended minimum separator diameter: electrode diameter + 2mm (max. 22 mm)
maximum electrode sandwich thickness: 2.5 mm 
operating temperature: -40°C – 80°C

Pt100 temperature sensor specification:
sensor type: Pt100 (100 Ohms @ 0°C) to IEC 751, Class B, 4 wire
construction: 3 mm diameter, 316 stainless steel sheath
probe temperature range: -50°C to +250°C
extension cable: 2 metre flexible Teflon® insulated, screened
termination: 4-wire tails – allows connection to any PT100 instrument 2, 3 or 4 wire (on request DB9 connector can be included)

Product includes 
1 x three-electrode cartridge with temperature sensor port
1 x Pt100 temperature sensor
1 x punch-type reference electrode  
1 x upper plunger (Stainless Steel 316L/317L) 
1 x lower plunger (Stainless Steel 316L/317L) 
1 x separator locking ring 
1 x set of O-Rings 
1 x temperature sensor mount