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ECD-4-nano

簡介

ECD-4-nano

Advanced Electrochemical Dilatometer for the measurement of electrode expansion with nanometer resolution.

  • Capacitive displacement sensor (range 250 μm, resolution better than 5 nm)
  • Additional gas pressure (0 to 3 bar) and temperature sensor (-20 to 80° C)
  • Cableless connection via PAT socket, with electronic cell tag (PAT-Button)
  • PRODUCT DETAILS

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Advanced test cell for the measurement of the electrode expansion in the nanometer range.
The ECD-4-nano takes dilatometry measurements to the next level
The ECD-4-nano is a high-resolution electrochemical dilatometer. The most powerful version offers a capacitive parallel plate sensor system with a resolution of better than 5 nanometers. This makes the ECD-4-nano the perfect instrument for detecting thickness changes of the individual electrode or the full cell stack during the electrochemical cycle.
The ECD-4-nano‘s completely redesigned test cell features a corrosion-resistant cell bottom and a new One-Seal concept that significantly improves tightness over previous ECD-3 models. This enables stable long-term operation as well as the use of a wide range of electrolytes.
To further improve workflow and handling, we have now integrated the ECD-4-nano into the PAT system. The dilatometer can be inserted directly into a PAT-Tester-x or a docking station such as the PAT-Clamp-1. This allows a space-saving and fast setup of the instrument. Needless to say, the integrated PAT-Button also ensures automatic recognition of the test cell in our EL-Software measurement software.
Sample Test Results


Sample Setup


Sample Setup

Working principle of the ECD-4-nano (3-electrode setup)
he working electrode (WE) and the counter electrode (CE) are separated by a stiff glass frit soaked with electrolyte. The upper WE is sealed by means of a flexible metal membrane, through which any charge-induced thickness change is transmitted towards the sensor/load unit attached on top. The fixation of the glass frit ensures that only the thickness change of the working electrode is being detected without interference from the CE.

Length 64 mm
Width 67 mm
Height 149 mm
Weight 2 kg  
Sample diameter 10 mm
Glass T-Frit (Separator) 12.5/10 x 3.5 mm
Separator diameter (full cell mode) max. 10 mm
Working (upper) electrode diameter max. 10 mm
Counter (lower) electrode diameter max. 12 mm
Gas pressure sensor: 0 to 3 bar abs.
Chemical compatibility Aprotic organic electrolytes
Cell electrolyte volume approx. 0.2 ml
Operational temperature range (cell and sensor) -20 to 80° C
Operational temperature range (conditioning electronics and data logger) 0 to 40 °C
Load on test specimen approx. 1 Newton
 
Product variants ECD-4-nano ECD-4
 
Displacement sensor type: Capacitive LVDT
Displacement range: 250 μm 500 μm
Displacement resolution: ≤ 5 nm ≤ 50 nm

 

Compatible PAT docking stations and potentiostats