描述 Complete Kelvin Probe是 Instytut Fotonowy 的一項發明,它解決了 Kelvin 探針 150 年來的老問題:如果您觀察到 CPD 變化,您不知道這是樣品的功函數(Work Function)變化,還是探針尖功函數(Work Function) 的變化。完整凱爾文探針(KelvinProbe)系統 是一款終極接觸電位差 (CPD) 測量裝置。它可以執行其它凱爾文探針所能執行的任何功能,而且還可以測量 :
這可讓使用者清楚看到樣品-探針尖 CPD 的貢獻來自於樣品,以及探針尖的貢獻。
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工作中的完整凱爾文探針
樣品-探針尖的 CPD 樣品尖端接觸電位差(藍色)與記錄的環境空氣溫度(綠色)和相對濕度(橘色): |
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樣品-接地 CPD 樣品-接地接觸電位差(紅色)與記錄的環境空氣溫度(綠色)和相對濕度(橙色)。 |
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探針尖-接地 CPD 探針尖與接地的接觸電位差(金色)與記錄的環境空氣溫度(綠色)和相對濕度(橘色)。 這顯示大部分的 CPD 變化都是由於探針尖表面的變化: |
凱爾文探針模組
凱爾文探針組包含 :
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凱爾文探針儀器配備:
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探針尖 凱爾文探針系統最重要的部分是探針尖。參考電極由直徑 2.5 mm 的金網格製成。 探針尖是完全由 Instytut Fotonowy Sp. z o.o. 設計和製造的元件。 |
樣品支架
標準凱爾文探針組包含兩種樣品支架:
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法拉第籠 整個儀器被法拉第籠所覆蓋,可將裝置與環境光線和電場隔離。 |
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氣密型法拉第籠與惰性氣體流動系統 由於 CPD 測量通常對環境因素(如溫度、濕度、灰塵和化學污染物)非常敏感,因此凱爾文探針可放置在帶有惰性氣流系統的密封型法拉第籠內。 |
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雷射屏障 凱爾文探針系統配備了雷射屏障系統。系統會自動偵測樣品基板。每次探針接近被檢測的樣品時,都會以 20 µm 的精度測量樣品表面與探針尖之間的精確距離。 |
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樣品照明 在測量過程中,樣品可能會被位於探針尖上方的光纖照亮。探針頭會讓光線穿過。光纖輸入端的光源可由 LED 迴轉燈、結合單色光的氙燈或任何其它類型的光源提供。 |
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由於儀器的不斷發展,以下參數可能會有所改變 | |
電壓範圍 | -5 V .. 5 V |
電壓測量標準解析度 | 0.15 mV |
測量技術 | 雙通道鎖相增強 |
樣品架 | X-Y位移平臺, 手動(預設)或電動 |
X-Y軸衝程 | 15 mm x 15 mm |
提示類型 | 網格, 直徑2.5 mm |
Z定位 | Z級電動 |
相對於樣本的定位 | 擋光板 |
Z定位解析度 | 10 µm |
Spectral range for wave guides | 200 nm .. 2000 nm(取決於波導) |
液體波導的選擇(Lumatec) | |
輔助感測器 | 濕度和溫度 |
內部法拉第籠照明 | 白色 LED |
X-Y定位輔助設備 | 激光放樣儀 |
電腦連接 | USB 2.0 |
尺寸 | 40 x 40 x 45 cm |
重量 | 10 kg |
Description
That lets the user clearly see what contribution to the sample-tip CPD comes from the sample and what from the tip. |
Complete Kelvin Probe at work
Sample-Tip CPD
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Sample-ground CPD |
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Tip-ground CPD Tip-ground Contact Potential Difference (gold) with recorded ambient air temperature (green) and relative humidity (orange). It shows that most of the CPD change is due to the change on the tips surface: |
kelvin probe modules
The Kelvin Probe set consists of:
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The Kelvin Probe instrument is equipped with:
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Probe Tip The Probe Tip is the component fully designed and manufactured by Instytut Fotonowy Sp. z o.o. |
Sample holders
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Faraday Cage The entire instrument is covered with the Faraday Cage, shielding the setup from the ambient light and electromagentic fields. |
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Gas-tight Faraday Cage with inert gas flow system Scince measurements of the CPD is often sensitive to environmental factors such as temperature, humidity, dust and chemical contaminants, Kelvin Probe may be placed inside the hermetic version of the Faraday Cage with the inert gas flow system. |
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Laser barrier The Kelvin Probe is equipped with the Laser barrier system. The system automatically detects the sample substrate. Each time the probe approaches the sample being examined, an accurate distance between the sample surface and the Probe Tip is measured with 20 µm precision. |
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Sample illumination The sample may be illuminated during the measurements from the optical fiber situated above the Probe Tip. The Probe Tip lets the light through. The light at optical fiber input may be provided by the LED Revolver, Xenon Lamp combined with the Monochromator or any other type of the light source desired. |
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Voltage range | -5 V .. 5 V |
Voltage measurement nominal resolution | 0.15 mV |
Measurement technology | 2-channel lock-in amplifier |
Sample holder | translation stage X-Y, manual (default) or motorized |
X-Y stage stroke | 15 mm x 15 mm |
Tip type | Au mesh, dia. 2.5 mm |
Tip Z positioning | motorized Z stage |
Positioning with respect to a sample | light barrier |
Tip Z positioning resolution | 10 µm |
Spectral range for wave guides | 200 nm .. 2000 nm (depending on a waveguide) |
Liquid waveguides selection (Lumatec) | |
Auxiliary sensors | humidity and temperature |
Internal Faraday cage illumination | white LED |
X-Y positioning aid | laser sample placement indicator |
PC connectivity | USB 2.0 |
Size | 40 x 40 x 45 cm |
Weight | 10 kg |